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電位滴定法檢測氟胞嘧啶含量
更新時間：2018-08-17瀏覽：2897次
氟胞嘧啶：抗真菌藥。
應用領域
醫藥
樣品
氟胞嘧啶樣品
檢測項目
氟胞嘧啶
參考標準
《中華人民共和國藥典》
儀器配置
儀器：CT-1Plus型電位滴定儀
電極：非水PH滴定電極
試劑選擇
滴定劑：高氯酸-冰醋酸溶液
溶劑：冰醋酸溶液
醋酸酐
方法
精密稱取氟胞嘧啶樣品約0.1g，置于干燥的滴定杯中，加冰醋酸20mL與醋酸酐10mL微熱溶解后，放冷，照電位滴定法，用高氯酸-冰醋酸溶液滴定，記錄消耗滴定劑的體積數。
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